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의료용 고분자 부문위원회
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Synthesis and Characterization of Crosslinkable Slide-ring Polyrotaxane based on β-Cyclodextrin (β-CD)
발표자

한서영 (부산대학교)

연구책임자

정일두 (부산대학교)

공동저자
한서영 (부산대학교), 최지운 (부산대학교), Rudru gangaratnamma (부산대학교), 정일두 (부산대학교)

초록

내용
This study aims to develop a novel movable crosslinked 3D network structure by using supramolecular movable polyrotaxane as a mobile crosslinker. Polyrotaxane was synthesized by threading β-cyclodextrin (β-CD) onto a poly(propylene glycol) bis(2-aminopropylether) (PPG-NH2, Mn=4000) chain, followed by end-capping with N-(triphenylmethyl)-glycine (Trt-Gly-OH) and DMT-MM as a catalyst. The slide-ring movement of threaded β-CDs on polyrotaxane enhanced mechanical properties including stress relaxation, tensile strength, and flexibility. To enable photopolymerization, polymerizable double bonds derived from methacryloyl chloride (MAC) were introduced onto the threaded β-CDs using triethylamine (TEA) as a catalyst. The synthesized polyrotaxane was characterized by ¹H-NMR, FT-IR, DSC and TGA.
발표코드
3PS-132
발표일정
2026-04-10  08:30 - 10:00